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题名	Rh-Catalyzed Asymmetric Hydrogenation of Unsaturated Medium-Ring NH Lactams: Highly Enantioselective Synthesis of N-Unprotected 2,3-Dihydro-1,5-benzothiazepinones
作者	Yin，Congcong1 ; Yang，Tao1 ; Pan，Yingmin1 ; Wen，Jialin1,2 ; Zhang，Xumu1
通讯作者	Wen，Jialin; Zhang，Xumu
发表日期	2020
DOI	10.1021/acs.orglett.9b04478
发表期刊	ORGANIC LETTERS 影响因子和分区
ISSN	1523-7060
EISSN	1523-7052
卷号	22 期号:3页码:920-923
摘要	A straightforward method to prepare 1,5-benzothiazepines was reported. Catalyzed by a Rh/Zhaophos complex, unsaturated cyclic NH lactams with a medium-size ring were hydrogenated smoothly, giving remarkably high enantioselectivities. The sulfur atom in the substrates did not bring an inhibition which was observed with commercially available bisphosphine ligands. This method was successfully applied in the scale-up synthesis of (R)-(-)-thiazesim.
相关链接	[Scopus记录]
收录类别	SCI ; IC ; CCR
语种	英语
重要成果	NI期刊 ; NI论文
学校署名	第一 ; 通讯
资助项目	Science, Technology, and Innovation Commission of Shenzhen[JCYJ20170817104350391] ; Science, Technology, and Innovation Commission of Shenzhen[KQTD20150717103157174]
WOS研究方向	Chemistry
WOS类目	Chemistry, Organic
WOS记录号	WOS:000513082700032
出版者	AMER CHEMICAL SOC
ESI学科分类	CHEMISTRY
来源库	Web of Science
引用统计	被引频次[WOS]：22
成果类型	期刊论文
条目标识符	http://kc.sustech.edu.cn/handle/2SGJ60CL/67913
专题	理学院_化学系前沿与交叉科学研究院深圳格拉布斯研究院
作者单位	1.Shenzhen Grubbs Institute,Department of Chemistry,Southern University of Science and Technology,Shenzhen, Guangdong,518055,China 2.Academy for Advanced Interdisciplinary Studies,Southern University of Science and Technology,Shenzhen, Guangdong,518055,China
第一作者单位	化学系; 深圳格拉布斯研究院
通讯作者单位	化学系; 深圳格拉布斯研究院; 前沿与交叉科学研究院
第一作者的第一单位	化学系; 深圳格拉布斯研究院
推荐引用方式 GB/T 7714	Yin，Congcong,Yang，Tao,Pan，Yingmin,et al. Rh-Catalyzed Asymmetric Hydrogenation of Unsaturated Medium-Ring NH Lactams: Highly Enantioselective Synthesis of N-Unprotected 2,3-Dihydro-1,5-benzothiazepinones[J]. ORGANIC LETTERS,2020,22(3):920-923.
APA	Yin，Congcong,Yang，Tao,Pan，Yingmin,Wen，Jialin,&Zhang，Xumu.(2020).Rh-Catalyzed Asymmetric Hydrogenation of Unsaturated Medium-Ring NH Lactams: Highly Enantioselective Synthesis of N-Unprotected 2,3-Dihydro-1,5-benzothiazepinones.ORGANIC LETTERS,22(3),920-923.
MLA	Yin，Congcong,et al."Rh-Catalyzed Asymmetric Hydrogenation of Unsaturated Medium-Ring NH Lactams: Highly Enantioselective Synthesis of N-Unprotected 2,3-Dihydro-1,5-benzothiazepinones".ORGANIC LETTERS 22.3(2020):920-923.